Reference List. 2. Binkowski, J. Skrócenie czasu oznaczania azotu w związkach organicznych metodą Dumasa. Chem Anal. 1972; 18:381.

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1 Reference List 1. Binkowski, J. Erreurs en microanalyse organique elementaire. Effet de la presence du chlore ou du brome. Pure & Appl Chem. 1972; 29:1. 2. Binkowski, J. Skrócenie czasu oznaczania azotu w związkach organicznych metodą Dumasa. Chem Anal. 1972; 18: Bodalski, R. and Pietrusiewicz, K. M. A new route to the phospholane ring-system. Tetrahedron Lett. 1972; 41: Chojnowski, J.; Stańczyk, W. A., and Kowalski, J. The cleavage of α-halogen substituted alkyl from silicon. I. Kinetics and mechanism of base-catalysed solvolysis of dichloromethyltrimethylsilane in protic solvents. Bull Pol Acad Sci Chem. 1972; XX: Kryszewski, M. Formation of supermolecular structures in thin polymers layers. Pure & Appl Chem. 1972; 31: Kryszewski, M.; Jabłoński, W., and Sapieha, S. Structure of single hole breakdown. Polarisation and conductivity insulating polymers; Bratysława. 1972: Kryszewski, M. and Pakuła, T. A study of the elongation ration of deformed spherulites. Polymer Symp. 1972; 38: Kryszewski, M.; Sapieha, S., and Cygler, M. On some electrical properties of thin polymer films. Polarisation and conductivity insulating polymers; Bratysława. 1972: Kubisa, P. and Słomkowski, S. Wpływ zasadowości monomerów na procesy polimeryzacji. Wiadomości Chemiczne. 1972; 26: Michalski, J. and Mikołajczyk, M. Stereochemia nukleofilnogo zamieshchenija u tiofosforilnogo centra. Khimia i Primienienije Fosforoorganicheskihk Sojedinienij. 1972( ). 11. Michalski, J. and Stec, W. J. Chemie und Stereochemie schwefel- und selenhaltiger organischer Phosphorverbindungen. Chemiker-Zeitung. 1972; 96: Mikołajczyk, M. and Drabowicz, J. Optically active O-alkyl alkylsulphinates. Tetrahedron Lett. 1972: Mikołajczyk, M. and Omelańczuk, J. 31 P NMR nonequivalence of (-)α-phenylethylammonium salts of chiral phosphorus thioacids. Tetrahedron Lett. 1972: Mikołajczyk, M.; Omelańczuk, J., and Para, M. Configuration of the optically active phosphorus thioacids. I. Chemical correlation of the configuration of O-alkyl alkylphosphonothioic acids. Tetrahedron. 1972; 28: Mikołajczyk, M.; Para, M.; Omelańczuk, J.; Kajtar, M., and Snatzke, G. Configuration of the optically active phosphorus thioacids. II. Chiroptical properties of O-alkyl alkylphosphonothioic acids and alkylphosphinothioic acids and their derivatives. Tetrahedron. 1972; 28: Mikołajczyk, M. and Łuczak, J. DMSO oxidations. A new method for the conversion of C=S and C=Se groups into a carbonyl group. Chem and Ind. 1972: Stereochemistry of organophosphorus cyclic compounds. I. Stereospecific synthesis of cis- and trans-2-hydroxy-2-thio(seleno)-4-methyl-1,3,2-dioxaphosphorinanes. Tetrahedron. 1972; 28: Nedkov, E.; Michajłov, M.; Kryszewski, M.; Milczarek, P., and Gałęski, A. Light scattering by large unit structures of poly-oxy-methylene-diacetate with and without additives. Vysokomol

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3 Eigenschaften. Plaste Und Kautschuk. 1973; 20: Kryszewski, M. Über die Diffusion von Komponenten in der Grenzflächenschichten von Polymermischungen. Plaste Und Kautschuk. 1973; 20: Zależność właściwości elektrycznych cienkich warstw wielkocząsteczkowych dielektryków organicznych od struktury. I Ogólnopolskie Sympozjum "Fizyka Cienkich Warstw"; Szczyrk. INTE; Kryszewski, M.; Gałęski, A.; Pakuła, T., and Grębowicz, J. Transport phenomena on interfaces in blends of polypropylene and polyethylene. J Colloid and Interface Science. 1973; 44: Kryszewski, M. and Nadolski, B. On the application of electron spectroscopy of photochromic substances to the determination of molecular interaction. Adv in Molecular Rel Proc. 1973; 6: Kryszewski, M.; Sapieha, S., and Nadolski, B. Electrical conduction of photochromic substances in polymeric matrices. Perlman, M. M. Elect. charge storage and transport in dielectrics. Princenton: The Electrochem Soc; 1973; p Kubisa, P. and Penczek, S. Reversible cationic copolymerization of heterocyclic monomers above the ceiling temperature. Part II. Tetrahydrofuran-oxetanes systems. Roczniki Chemii. 1973; 47: Mikołajczyk, M. and Drabowicz, J. Organosulfur compounds. I. Magnetic non-equivalence and optical activity in amidosulfites. Sulfur Chemistry Part A. 1973; 8: Mikołajczyk, M. and Omelańczuk, J. Configuration of the optically active phosphorus thioacids-iii. Synthesis and optical resolution of O-methyl isopropylphosphonothioic acid. Phosphorus. 1973; 3: Mikołajczyk, M. and Zatorski, A. Organosulfur compounds. II. α-phosphorylsulfoxides. I. Synthesis. Synthesis. 1973: Mikołajczyk, M. and Zatorski, A. Part II. Organosulfur compounds. α-phosphorylsulphoxides I: Synthesis. Synthesis. 1973: Pakuła, T.; Gałęski, A., and Kryszewski, M. Study of deformation of a single spherulite. J Polym Sci: C. 1973; 42: Penczek, S. Polimeryzacja. Polimery. 1973: Penczek, S.; Fejgin, J.; Kubisa, P.; Matyjaszewski, K., and Tomaszewicz, M. New highly efficient initiators for the polymerization of 1,3-dioxolane with 1,3,5-trioxane based on the derivatives of trifluoromethanesulfonic acid. Makromol Chem. 1973; 172: Penczek, S. and Kubisa, P. Kinetics and mechanism of cyclic acetals polymerization initiated by stable carbonium salts II. Confirmation of the initiation mechanism for triphenylmethyl hexachloroantimonate in the polymerization of 1,3-dioxolan. Makromol Chem. 1973; 165: Penczek, S. and Słomkowski, S. Kinetics of the nonstationary polymerization involving polymer in the initiation step. Bull Pol Acad Sci Chem. 1973; 21: Piechucki, C. and Michalski, J. 1,2-Cyclopropane ring cleavage in the reactions of 1-cyano-1-(2 ' -pyridyl)-2-alkyl(aryl)cyclopropanes with hydrochloric acid. Bull Pol Acad Sci Chem. 1973; 6: Piechucki, C. and Michalski, J. Preparation of secondary and tertiary ß-(2-pyridyl)-alkanols. Synthesis.

4 1973: Saenger, W. and Mikołajczyk, M. Kristall- und Molekulstruktur des 2-Hydrogen-2-Oxo-4-Methyl-1,3,2-Dioxaphosphorinanes. Eine P-H...O-wassersto. Chem Ber. 1973; 106: Skowrońska, A. Stereochemistry of oxidation of trivalent phosphorus compounds with ozone and m-chlorobenzoic acid. Bull Pol Acad Sci Chem. 1973; 6: Skowrońska, A.; Mikołajczak, J., and Michalski, J. Diastereoizomeric 2-chlorothio-2-oxo-4-methyl-1,3,2-dioxaphosphorinans. Bull Pol Acad Sci Chem. 1973; 6: Stec, W. J. Organophosphorus compounds of sulfur and selenium. Stereochemistry of silver-ion promoted solvolysis of some halogenoanhydrides and thioloesters of organophosphorus acids. Bull Pol Acad Sci Chem. 1973; 21: Stec, W. J. and Mikołajczyk, M. Stereochemistry of organophosphorus cyclic compounds II. Stereospecific synthesis of cis- and trans-2-halogeno-2-oxo-4-methyl-1,3,2-dioxaphosphorinans and their chemical transformations. Tetrahedron. 1973; 29: Stec, W. J.; Okruszek, A., and Michalski, J. Stereochemistry of oxidation of P(III) compounds with amine N-oxides. Equatorial preference of N,N-dimethyloamino group in 4-methyl-1,3,2-dioxaphosphorinanyl ring system. Bull Pol Acad Sci Chem. 1973; 21: Stec, W. J.; Uznański, B., and Michalski, J. Assignment of the cis-trans geometry in diastereomeric 2-thiono- and 2-seleno-2-hydrogen-4-methyl-1,3,2-dioxaphosphorinans. Phosphorus. 1973; 3: The synthesis and stereochemical transformations of 2-hydrogen-4-methyl-1,3,2-diooxaphosphorinan. Phosphorus. 1973; 3: Stec, W. J. and Łopusiński, A. Stereochemistry of organophosphorus cyclic compounds. III. The stereospecific synthesis of cis- and trans-2-n-phenylamino-2-oxo-4-methyl-1,3,2-dioxaphosphorinans. Tetrahedron. 1973; 29: Urbański, T.; Kryszewski, M.; Kosiński, K., and Sas, W. Charge transfer in simple organic compounds. Roczniki Chemii. 1973; 47: Binkowski, J. Badania nad automatyzacją grawimetrycznej metody oznaczania węgla i wodoru. I. Chem Anal. 1974; 19: Binkowski, J. and Rudnicki, A. Analiza elementarna związków fosforoorganicznych. VI. Grawimetryczne oznaczanie węgla i wodoru. Chem Anal. 1974; 19: Blackburne, L. D.; Katritzky, A. R.; Read, D. M.; Bodalski, R., and Pietrusiewicz, K. M. The conformational analysis of saturated heterocycles. part LXII. Cis-trans-equilibria of 4-phospha-analogues of 2,6-dimethylonecyclohexanon. J Chem Soc Perkin : Bluj, S.; Borecka, B.; Łopusiński, A., and Michalski, J. Synthesis of dineopentoxyoxophosphoranesulfenyl chloride and some other organic phosphorus derivatives with neopentoxy group. Roczniki Chemii. 1974; 48: Borecka, B.; Jezierska, B.; Bluj, S., and Michalski, J. Synthesis and chemical properties of dialkoxyoxophosphorane sulphenates (RO) 2P(O)-S-OR. Bull Pol Acad Sci Chem. 1974; 21:

5 68. Chojnowski, J.; Mazurek, M.; Ścibiorek, M., and Wilczek, L. Cationic polymerization of siloxanes-approach to the mechanistic studies. Makromol Chem. 1974; 175: Chojnowski, J. and Stańczyk, W. A. Cleavage of α-halosubstituted alkyl groups from silicon. The effect of halogen in the base-catalysed solvolysis of /α-dihalogeno-methyl/ trimethylsilanes. J Organomet Chem. 1974; 73: Gałęski, A. and Kryszewski, M. Small angle light scattering from hedrites, ovoids and spiral ovoids. I. Theoretical consideration. J Polym Sci B: Polym Phys. 1974; 12: Small angle light scattering from hedrites, ovoids and spiral ovoids. II. Experimental. J Polym Sci B: Polym Phys. 1974; 12: Gloede, J.; Mikołajczyk, M.; Łopusiński, A., and Omelańczuk, J. Darstellung von reinen Phosphorigsäure-Diäthylester-Chlorid. Journal Für Praktische Chemie. 1974; 316: Kowalski, J.; Chojnowski, J.; Stańczyk, W. A., and Mazurek, M. Oznaczanie zawartości cyklicznych oligomerów w polidwumetylosiloksanie, metoda chromatografii gazowej z zastosowaniem detektora płomieniowo-jonizującego. Polimery. 1974; 19: Krawiecka, B.; Michalski, J.; Mikołajczak, J.; Mikołajczyk, M.; Omelańczuk, J., and Skowrońska, A. Stereochemistry of desulphurisation and deoxygenation of oxophosphoranesulphenyl chlorides by trivalent phosphorus compounds. J Chem Soc Chem Commun. 1974: Krawiecka, B.; Michalski, J., and Skrzypczyński, Z. The stereochemistry of acid - catalysed solvolysis at sterically hindered thiophosphoryl centre. J Chem Soc Chem Commun. 1974: Kryszewski, M. Electrical properties of amorphous and semicrystalline organic solids. "Elektryczne Własności Organicznych Ciał Stałych"; Karpacz. Wyd. Politechniki Wrocławskiej; 1974: Fizyka polimerów. Polimery. 1974; 19: Kryszewski, M.; Gałęski, A.; Jabłoński, W., and Sapieha, S. Formation of supermolecular structure in thin polymer films. Polymer. 1974; 15: Kryszewski, M.; Gałęski, A., and Milczarek, P. Bestimmung von Größe und Struktur der in Polymeren enstehenden Sphärolithzentren. Plaste Und Kautschuk. 1974; 2: Kryszewski, M. and Nadolski, B. Some relations between iodine swelling in polyacrylomitryle films and their preparation techniques. Roczniki Chemii. 1974; 48: Kryszewski, M.; Pakuła, T., and Grębowicz, J. Nadmolekularnaja struktura smiesiej polipropylena s polietylenom. Vysokomol Soedin. 1974; 16A: Kryszewski, M.; Sapieha, S.; Tyczkowski, J., and Zieliński, M. Electrical and photoelectrical properties of glassy photochromic substances. Elektryczne własności organicznych ciał stałych; Karpacz. Wyd. Politechniki Wrocławskiej; 1974: Malinowski, R. and Mikołajczyk, M. The synthesis and investigation of some insecticidally active enolphosphonates. Prace IPO. 1974; 6: Matyjaszewski, K.; Kubisa, P., and Penczek, S. Ion-ester equilibrium in the living cationic polymerization of tetrahydrofuran. J Polym Sci A: Polym Chem. 1974; 12: Matyjaszewski, K. and Penczek, S. Comments on the paper: "NMR studies on the polymerization of cyclic ethers" by Pruckmayer and T. K. Wu. Macromolecules. 1974; 7: The macroester-macroion equilibrium in the cationic polymerization of THF observed directly by

6 300 MHz 1 H NMR. J Polym Sci A: Polym Chem. 1974; 12: Michalska, M.; Michalski, J., and Orlich, I. Glycosylation of organic thio- and selenoacids of phosphorus. Bull Pol Acad Sci Chem. 1974; 22: Michalski, J.; Młotkowska, B., and Skowrońska, A. Organophosphorus compounds. Part CL. Synthesis of "stable" tetra-o-alkyl sym-monothiopyrophosphates. J Chem Soc Perkin : Mikołajczyk, M. and Drabowicz, J. Asymmetric synthesis of amidothiosulphites. Substitutions at sulphur with retention of configuration. J Chem Soc Chem Commun. 1974: Asymmetric synthesis of sulphinic sters with sulphur atom as a sole chirality centre. J Chem Soc Chem Commun. 1974: Organosulfur compounds. III. One-step synthesis of alkyl tert-alkanesulfinates. Synthesis. 1974: Mikołajczyk, M.; Krzywański, J., and Ziemnicka, B. Synthesis of the diastereomerically pure trans-2-halogeno-4-methyl-1,3,2-dioxaphosphorinan-2-thiones and conforamtional studies. Phosphorus. 1974; 5: Mikołajczyk, M. and Łuczak, J. Dimethyl sulphoxide oxidations: a general method for the conversion of a thio- or selenophosphoryl group into a phosphoryl group. Chem and Ind. 1974: Dimethyl sulphoxide oxidations: a new selective conversion of the thiocarbonyl-containing nucleic acid components into their oxygen analogues. Synthesis. 1974: Pakuła, T.; Gałęski, A., and Kryszewski, M. Wyznaczanie rozkładu rozmiarów cząsteczek zawiesin. I. Metaoda wyznaczania rozkładu rozmiarów cząsteczek. Chem Anal. 1974; 19: Pakuła, T.; Kryszewski, M.; Grębowicz, J., and Gałęski, A. Two-dimensional model of mechanical properties of polymer blends: application to polypropylene and polyethylene blends. Polymer J. 1974; 6: Pakuła, T. and Soukup, Z. New apparatus for studies on supermolecular structures of thin polymer films by salts. J Polym Sci B: Polym Phys. 1974; 12: Penczek, S. Aktualne problemy polimeryzacji kationowej. Polimery. 1974: Hydride ion transfer process and cationic polymerization of cyclic acetals. Makromol Chem. 1974; 175: Sapieha, S.; Jabłoński, W., and Kryszewski, M. The structure of incomplete destructive breakdown spots in thin polymer films. Electro-Component Science and Technology. 1974; 1: Sapieha, S. and Kryszewski, M. Elektryczna i optyczna stymulacja przebić w cienkich warstwach dielektryków. Archiwum Elektroniki. 1974; 23: Stec, W. J. Heteronuclear spin-spin coupling constans between directly bonded atoms as a probe of configuration at phosphorus atom involved in diastereoisomeric 4-methyl-1,3,2-dioxaphosphorinans. Z Naturforsch. 1974; 19b: Stec, W. J.; Konopka, A., and Uznański, B. Synthesis of a dialkyl phosphoroisocyanidate. J Chem Soc Chem Commun. 1974: Stolarczyk, A.; Kubisa, P., and Penczek, S. Ion association and free ion formation effects on the 1 NMR parameters of 1,3-dioxolan-2-ylium salts in the polymerization of 1,3-dioxolan. Bull Pol Acad Sci Chem. 1974; 22:431.

7 105. Słomkowski, S. and Penczek, S. The carbenium-oxonium ion equilibrium. Part I. Reversible reaction on non-paired triphenylmethyl cation with ethers and acetals. J Chem Soc Perkin : Wróbel, A. M. and Kryszewski, M. The structure and thermal stability of glow discharge polysilazane. Bull Pol Acad Sci Chem. 1974; 23: Łapienis, G. and Penczek, S. Kinetics and thermodynamics of the polymerization of the cyclic esters of phosphoric acid II. Cationic polymerization of 2-metoxy-2-oxo-1,3,2-dioxaphosphorinane 1,3-propylene methyl phosphate. Macromolecules. 1974; 7: Bartczak, T. J.; Christensen, A.; Kinas, R., and Stec, W. J. Cis-2-t-butylamino-2-seleno-4-methyl-1,3,2-dioxaphosphorinan, C 8H 18NO 2PSe. Crystal Structure Commun. 1975; 4: Bartczak, T. J.; Christensen, A.; Kinas, R., and Stec, W. J. Synthesis and cis-trans-geometry assignment in diastereoisomeric 2-t-butylamino-4-methyl-1,3,2-dioxaphosphorinans and their 2-seleno derivatives. Tetrahedron Lett. 1975: Bodalski, R.; Pietrusiewicz, K. M., and Koszuk, J. A new synhesis of 2-phospholene-1-oxides. Reaction of sec-benzylphosphine oxides and related compounds with α, β - unsaturated ketones. Tetrahedron. 1975; 31: Borecka, B.; Jezierska, B., and Michalski, J. Synthesis, chemical properties and stereochemistry of oxophosphorane-sulphenates. Organic Sulphur Chemistry. 1975: Chojnowski, J. and Mazurek, M. Anionic polymerization of siloxanes-mechanism of initiation with triorganosilanolates. Makromol Chem. 1975; 176: Anionnaja polimerizacija cikliczeskich siloksanow. Kinetika iniciirowanija polimerizacji gieksametilciklotrisiloksana fenildimetil silanolatom kalija. Advances in Anionic Polymerization. 1975: Chojnowski, J. and Stańczyk, W. A. Cleavage of α-halosubstituted alkyl groups from silicon. The mechanism of catalysis by ammonia buffer. J Organomet Chem. 1975; 99: Degórski, A. and Kryszewski, M. Transfer of excitation energy in rigid solutions containing charge - transfer complexes. I. Quenchińg of fluorescence. J Chem Soc Faraday ; 71: Degórski, A. and Kryszewski, M. Transfer of excitation energy in rigid solutions containing charge - transfer complexes. II. Photoconductivity. J Chem Soc Faraday ; 71: Ishmaeva, E. A.; Mikołajczyk, M.; Remisov, A., and Pudovik, A. Conformation of P(O)SCH 3 and P(O)SeCH 3 groups in 1,3,2-dioxaphosphorinans. Dokłady Akademii Nauk. 1975; 223: Ishmaeva, E. A.; Mikołajczyk, M.; Remisov, A., and Pudovik, A. Issledovanie konformatsii P(O)SCH 3 i P(O)SeCH 3 grupp v 1,3,2-dioksa-fosforinanakh. Dokl Acad Nauk SSSR, Khimia. 1975; 223: Kałużyński, K.; Libiszowski, J.; Łapienis, G., and Penczek, S. Kinetika i termodinamika ravnoviesnoj kationnoj polimerizacji cikliczeskich efirow fosfornoj kisłoty. Adv Ionic Polym. 1975: Kinas, R.; Pankiewicz, K., and Stec, W. J. The synthesis of enantiomeric cyclophosphamides. Bull Pol Acad Sci Chem. 1975; 23: Kryszewski, M.; Gałęski, A.; Pakuła, T., and Grębowicz, J. Supermolecular structures in mixtures of polypropylene and polyethylene with and ethylne-propylene terpolymer. Sint Fiz Khim Polim. 1975; 1b:47.

8 122. Kryszewski, M. and Nadolski, B. Electrochromism of indolinobenzospirans dissolved in rigid amorphous polymer matrices. J Polym Sci A: Polym Chem. 1975; 12: Kubisa, P. and Vogl, O. Kationnaja polimerizacja chloralia. Vysokomol Soedin. 1975; 17: Lesiak, K.; Uznański, B., and Stec, W. J. Stereochemistry of the Michaelis-Backer reaction of cis- and trans-2-hydro-2-oxo-4-methyl-1,3,2-dioxaphosphorinan with methyl iodide. Phosphorus. 1975; 6: Markowska, A.; Michalski, J., and Olejnik, J. Reaction of triaryl phosphites with orthophosphoric and phosphonic acids. A general method of synthesis of arylphosphates and O-arylphosphonates. Bull Pol Acad Sci Chem. 1975; 23: Markowska, A.; Olejnik, J., and Michalski, J. Selective Alkylierung von mehrbasigen Säuren des 4-bindingen Phosphors mit Trialkylphosphit. Chem Ber. 1975; 108: Matyjaszewski, K.; Kubisa, P., and Penczek, S. Kinetics and mechanism of the cationic polymerization of tetrahydrofuran in solution I. THF-CCl n system. J Polym Sci A: Polym Chem. 1975; 13: Michalski, J. Chemistry and stereochemistry of organophosphorus compounds. Zjazd Japońskiego Towarzystwa Chemicznego; 1975: Chemistry and stereochemistry of selenium phosphorus compounds. Chem Scripta. 1975; 8A: Michalski, J. and Orlich, I. Base - catayzed intramolecular cyclization of β-keto-n-benzylnitrones. Synthesis of flawono[3,4-d]oxazoles. Bull Pol Acad Sci Chem. 1975; 23: Michalski, J. and Skrzypczyński, Z. Stereoselective deselenisation of tert-butylphenylphosphinoselenoic acids. Stereochemical relationship between tert-butylphenylphosphinoselenoic acids and their sulphur analogues. J Organomet Chem. 1975; 97 :C31-C Mikołajczyk, M.; Drabowicz, J.; Omelańczuk, J., and Fluck, E. Optically active trivalent phosphorus acid esters: an approach by asymmetric synthesis. J Chem Soc Chem Commun. 1975: Mikołajczyk, M.; Gajl, M., and Reimschüssel, W. Chlorine isotopic exchange at sulphur on sulphonyl chlorides. Accelerationg effect of the ortho-alkyl groups. Tetrahedron Lett. 1975: Mikołajczyk, M.; Grzejszczak, S.; Midura, W. H., and Zatorski, A. Organosulfur compounds. VII. Synthesis of α,β-unsaturated sulphides, sulphoxides and sulphones by the Horner-Witting reaction in two-phase system catalyzed by quaternary ammonium salts and crown ethers. Synthesis. 1975: Mikołajczyk, M.; Grzejszczak, S., and Zatorski, A. Organosulfur compounds. VI. α-phosphoryl-sulfoxides II. Synthesis of α,β-unsaturated sulfoxides and configurational assignments to geometrical isomers. J Org Chem. 1975; 40: Mikołajczyk, M.; Grzejszczak, S.; Zatorski, A.; Montanari, F., and Cinquini, M. α-phosphoryl sulphoxides and sulphones: new catalyst in two-phase alkylation of ketones. Tetrahedron Lett. 1975: Mikołajczyk, M.; Krzywa ński, J., and Ziemnicka, B. Diastereoisomeric 2-fluoro-4-methyl-1,3,2-dioxaphosphorinan-2-thiones. Retention stereochemistry in nucleophilic substitution at thiophosphoryl phosphorus. Tetrahedron Lett. 1975: Mikołajczyk, M. and Leitloff, M. Stereokhimia optitcheski aktivnikh tiokislot fosfora. Usp Chim. 1975; XLIV:1419.

9 139. Mikołajczyk, M. and Łuczak, J. Dimethyl sulphoxide oxidations: an iodine catalysed conversion of thio- or selenophosphoryl and carbonyl compounds into their oxygen analogues. Synthesis. 1975: Okruszek, A. and Stec, W. J. Axial preference of metylthio- substituent in dioxaphosphorinanyl ring system. Z Naturforsch. 1975; 30b: Omelańczuk, J.; Kiełbasiński, P.; Michalski, J.; Mikołajczak, J.; Mikołajczyk, M., and Skowrońska, A. Reaction of oxophosphoranesulphenyl chlorides with phosphorus trichloride. A new synthesis of dialkyl phosphorochloridothionates and their optically active analogues. Tetrahedron. 1975; 31: Penczek, S. Wpływ budowy anionu na kinetykę reakcji elementarnych w kationowej polimeryzacji heterocyklicznych monomerów. Adv Ionic Polym. 1975: Skowrońska, A.; Mikołajczak, J., and Michalski, J. Five-coordinate and phosphonium intermediates in reactions of phosphorus thionoesters =P(S)OR with elemental chlorine and sulfuryl chloride. J Chem Soc Chem Commun. 1975: Pentacovalent intermediate in the Arbuzow reaction. J Chem Soc Chem Commun. 1975: Stec, W. J.; Lesiak, K.; Mielczarek, D., and Stec, B. Assignment of cis-trans geometry in diastereoisomeric 2-benzyl-4-ethyl-1,3,2-dioxaphosphorinans and their 2-oxo- and 2-seleno derivatives. Z Naturforsch. 1975; 30b: Stec, W. J.; Lesiak, K., and Sudol, M. Reaction of carbonyl isothio(seleno)cyanates with trivalent phosphorus esters. Synthesis. 1975: Stec, W. J. and Okruszek, A. Axial preference of a 2-anilino substituent in 4-methyl-1,3,2-dioxaphosphorinan. J Chem Soc Perkin : Stec, W. J.; Sudoł, T., and Uznański, B. Deselenization of dialkyl phosphoroisoselenocyanatidite. J Chem Soc Chem Commun. 1975: Stec, W. J.; Uznański, B.; Houalla, D., and Wolf, R. Sur quelques reactions du dineopentoxyphosphanne. C R Acad Sci Paris. 1975; C-727: Stec, W. J.; Zielińska, B., and Van Wazer, J. R. Electron impact induced rearrangement of organic hypophosphates. Org Mass Spectrom. 1975; 10: Słomkowski, S. and Penczek, S. Kinetika i mechanizm pierienosa H - aniona k swobodnym Pn 3C + kationom w inicirowanii kationowoj polimerizacji. Adv Ionic Polym. 1975: Uznański, B. and Stec, W. J. Synthesis of dialkyl phosphorocyanidates. Axial preference of the P-cyano group in the dioxaphosphorinane ring system. Synthesis. 1975: Łopusiński, A. and Michalski, J. The cyanide cleavage of bis-phosphinyl disulphides. Chemistry of phosphinylthio- and isothiocyanates. Bull Pol Acad Sci Chem. 1975; 23: Łopusiński, A.; Michalski, J., and Stec, W. J. Ein neuer Weg zu Phosphor- und Phosphinocyanatidaten. Angew Chem. 1975: Stereochemistry of thiocyano-isothiocyano rearrangement P(O)SCN P(O)NCS in 2-oxo-4-methyl-1,3,2-dioxaphosphorinanyl ring system. Bull Pol Acad Sci Chem. 1975; 23: Synthesis and properties of diastereoisomeric 2-isothiocyano-2-oxo-4-methyl-1,3,2-dioxaphosphorinans. The role of nucleophilic catalysis in their epimerisation. Bull Pol Acad Sci Chem. 1975; 23:

10 157. Bartczak, T. J.; Christensen, A.; Kinas, R., and Stec, W. J. Trans-2-t-butylamino-2-seleno-4-methyl-1,3,2-dioxaphosphorinan, C 8H 18NO 2PSe. Crystal Structure Commun. 1976; 5: Binkowski, J.; Giziński, S.; Kamiński, R., and Reimschüssel, W. Untersuchung des Verhaltens der bei der Verbennung phosphoroorganischer Verbindungen entstehenden P-oxide und ihrer Absorption an geeigneten Substanzen mittels 32 P-markierten Verbindungen. I. Mikrochim Acta. 1976: Bukowska-Strzyżewska, M.; Dobrowolska, W.; Michalski, J.; Młotkowska, B., and Skoweranda, J. Crystal data for some bicyclic organic pyrophosphates and thiopyrophosphates. Roczniki Chemii. 1976; 50: Bukowska-Strzyżewska, M.; Michalski, J.; Młotkowska, B., and Skoweranda, J. The crystal and molecular structures of bis(5,5'-dimethyl-2-oxo-1,3,2-dioxa-phosphorinanyl)sulphide. Acta Crystallogr. 1976; B32: Buyle, A.; Matyjaszewski, K., and Penczek, S. Neighbouring group participation in the kinetics of the macroester-macroion pair interconversion in the cationic polymerization of THF. J Polym Sci Polym Lett Ed. 1976; 14: Chojnowski, J.; Mazurek, M., and Wilczek, L. Spectrophotometric microdetermination of silicon-bonded hydrogen with carbenium ion reagents. Analyst. 1976; 101: Chojnowski, J. and Ścibiorek, M. Cationic polymerization of siloxanes - kinetically controlled oligomerization in hexamethylcyclotrisiloxane /D 3/ - linear dimethylsiloxane systems. Makromol Chem. 1976; 177: Cox, P. J.; Farmer, P. B.; Jarman, M.; Jones, M.; Stec, W. J., and Kinas, R. Observations on the differential metabolism and biological activity of the optical isomers of cyclophosphamide. Biochem Pharm. 1976; 25: Davies, A. G.; Parrott, M. J.; Roberts, B., and Skowrońska, A. An electron spin resonance study of phosphoranyl radicals derived from tetra-alkyl esters of phosphorous phosphoric anhydride (RO) 2POP(O)(OR) 2. J Chem Soc Perkin : Drabowicz, J. and Mikołajczyk, M. Organosulfur compounds. XI. A mild and efficient reduction of sulphoxides by means of lithium alanate of titanium (IV) chloride. Synthesis. 1976: Fejgin, J.; Penczek, S., and Tomaszewicz, M. Usieciowane poliacetale. Polimery. 1976: Franta, E.; Reibel, L.; Lehman, J., and Penczek, S. Use of mono- and multifunctional oxocarbenium salts in the polymerization of THF. J Polym Sci Polym Symp. 1976; 56 : Gałęski, A. and Kryszewski, M. Small angle light scattering from square and hexagonal hedrites. J Polym Sci B: Polym Phys. 1976; 14: Ishmaeva, E. A.; Witczak, M.; Mikołajczyk, M., and Pudovik, A. Conformation of the P(O)SCH 3 and P(O)OSiMe 3 groups in 1,3,2-dioxaphosphorinanes. Izvestia Akad Naul SSSR, Ser Khim. 1976: Kałużyński, K.; Libiszowski, J., and Penczek, S. A new class of synthetic polyelectrolytes acidic polyesters of phosphoric acid. Macromolecules. 1976; 9: Kowalski, J. and Lasocki, Z. N,N-bis/halogenomethyl-dimethylsilyl/acetamides and their reactivity. J Organomet Chem. 1976; 116 : Kryszewski, M. and Ciesielski, W. Electrical and magnetic properties of complexes of TCNQ anion radical salt

11 III. The class trensition and crystallinity of complexes. Roczniki Chemii. 1976; 50: Electrical and magnetic properties of complexes of TCNQ anion radical salts. I. Electrical properties. Roczniki Chemii. 1976; 50: Electrical and magnetic properties of complexes of TCNQ anion radical salts. II. Magnetic properties. Roczniki Chemii. 1976; 50: Kryszewski, M.; Gałęski, A., and Milczarek, P. Destruction of polymers with crystalline unhomogeneities under the influence of intense laser beam. J Polym Sci Polym Lett Ed. 1976; 14: Kryszewski, M.; Nadolski, B., and Fabrycy, A. The photochromic effect of solid mercury dithiozonate solutions in macromolecular amorphous polymeric matrices. Roczniki Chemii. 1976; 49: Kubisa, P. Ion-ester equilibria in the polymerization of 1,3-dioxolane initiated by triphenylmethylium salts. Bull Pol Acad Sci Chem. 1976; Michalski, J.; Radziejewski, C., and Skrzypczyński, Z. Evidence for a sulphene intermediate in the base hydrolysis of the methanesulphonic anhydrides of phosphinothioic acids. J Chem Soc Chem Commun. 1976: Michalski, J.; Łopusiński, A.; Stec, W. J., and Fluck, E. Inhibitor-Effect von BF 3 auf die Umlagerung von O=P SCN in O=P NCS. Z Naturforsch. 1976; 31B: Mikołajczyk, M.; Costisella, B.; Grzejszczak, S., and Zatorski, A. Synthesis of O,S-thioacetals of formylphosphonates. Tetrahedron Lett. 1976: Mikołajczyk, M. and Drabowicz, J. Asymmetric reduction of chiral sulfoxides by optically active lithium aluminium hydride complexes with alcohols. Phosphorus, Sulfur and Silicon. 1976; 1: Optically stable thiosilphinate S-esters: asymmetric synthesis and nucleophilic substitution at sulphinyl sulphur. J Chem Soc Chem Commun. 1976: Mikołajczyk, M.; Drabowicz, J., and Bujnicki, B. Acid-catalysed conversion of sulphinamides into sulphinates. A new synthesis of optically active sulphinates. J Chem Soc Chem Commun. 1976: Mikołajczyk, M.; Grzejszczak, S.; Midura, W. H., and Zatorski, A. Organosulfur compounds. X. Horner-Witting reaction in two-phase system in the absence of a typical phase-transfer catalyst. Synthesis. 1976: Mikołajczyk, M.; Grzejszczak, S., and Zatorski, A. Organosulfur compounds. IX. NMR and structural assignments in α,β-unsaturated sulphoxides using additive increments method. Tetrahedron. 1976; 32: Mikołajczyk, M.; Grzejszczak, S.; Zatorski, A., and Młotkowska, B. A new general synthesis of ketene thioacetals. Tetrahedron Lett. 1976: Mikołajczyk, M.; Kiełbasiński, P., and Schiebel, H. M. Organosulfur compounds VIII. Reaction of monothiocarboxylic acids with dicyclohexylcarbodiimide and other reactions leading to monothioanhydrides. J Chem Soc Perkin : Mikołajczyk, M.; Witczak, M.; Wieczorek, M. W.; Bokij, N. G., and Struchkov, Y. T. Stereochemistry of organophosphorus compounds. IV. Synthesis and geometrical isomerism in cyclic five-membered phosphorus thioacids. Crystal and molecular structure of imidazolium salt of cis-2-hydroxy-4-methyl-1,3,2-dioxaphospholan-2-thione. J Chem Soc Perkin :371.

12 190. Okruszek, A. Procesy permutacyjnej izomeryzacji połączeń pięciowiązalnego fosforu. Wiadomości Chemiczne. 1976; 30: Okruszek, A. and Stec, W. J. The axial preference of fluorine atom in 2-fluoro-4-methyl-1,3,2-dioxaphosphorinanyl ring sytem. Z Naturforsch. 1976; 31b: Omelańczuk, J. and Mikołajczyk, M. Stereochemistry of nucleophilic substitution at the optically active trivalent phosphorus atom. J Chem Soc Chem Commun. 1976: Pakuła, T. and Kryszewski, M. Determination of the temperature depedence of spherulite growth rate in low density polyethylene using the small angle light scatering. Europ Polym J. 1976; 12: Pakuła, T.; Kryszewski, M., and Pluta, M. The dynamic of spherulite deformation in relation to the morphological parameters. Polymer Preprints. 1976; 17: Pakuła, T.; Kryszewski, M., and Soukup, Z. Determination of spherulite size distribution by small angle light scattering. Europ Polym J. 1976; 12: Penczek, S. Polymerization of cyclic ethers of phosphoric acid. Pure & Appl Chem. 1976; 48: Penczek, S. and Matyjaszewski, K. Ions and macroesters in the living cationic polymerization of THF. J Polym Sci Polym Symp. 1976; 56: Stańczyk, W. A. and Chojnowski, J. Cleavage of α-halosubstituted alkyl groups from silicon. general base catalysis in silicon-carbon bond cleavage. J Organomet Chem. 1976; 117: Stec, W. J.; Kinas, R., and Okruszek, A. Configurational assignments to 2-X-2-Y-4-methyl-1,3,2-dioxaphosphorinans. Z Naturforsch. 1976; 31b: Stec, W. J. and Lesiak, K. A novel route to 1-aminoalkylphosphonic acids. J Org Chem. 1976; 41: Stec, W. J.; Okruszek, A.; Lesiak, K.; Uznański, B., and Michalski, J. New synthesis of S(Se)-alkylphosphorothio(seleno)lates from the corresponding phosphoroanilidates. Stereospecific cleavage of the phosphorus-nitrogen bond in chiral phosphoroanilidates. J Org Chem. 1976; 41: Stec, W. J.; Okruszek, A., and Michalski, J. Organophosphorus compounds of sulfur and selenium. Stereochemistry of oxidation of thiono- and selenophosphoryl compounds with hydrogen peroxide. J Org Chem. 1976; 41: Stec, W. J.; Uznański, B.; Bruzik, K. B., and Michalski, J. Protic acid catalyzed thiono-thiolo rearrangements of phosphorus esters. J Org Chem. 1976; 41: Szymański, R.; Wieczorek, H.; Kubisa, P., and Penczek, S. New synthetic route to trialkyloxonium salts: alkylation of ethers. J Chem Soc Chem Commun. 1976: Słomkowski, S. and Penczek, S. Influence of dibenzocrown ether on the kinetics of anionic polymerization of propiolactone. Macromolecules. 1976; 9: Wieczorek, M. W.; Karolak-Wojciechowska, J.; Goliński, B.; Bartczak, T. J.; Mikołajczyk, M., and Witczak, M. Imidazolium salt of DL-2-hydroxy-4,5-dimethyl-1,3,2-dioxaphospholan-2-thione. C 7H 13NO 2O 3PS. Crystal Structure Commun. 1976: Wróbel, A. M.; Kryszewski, M., and Gazicki, M. Mechanism of polysilazane thin films formation during glow discharge polymerization of hexamethylcyclotrisilasane. Polymer. 1976; 17:673.

13 Structure of glow discharge polysilazane thin films. Polymer. 1976; 17: Zieliński, W. S.; Leśnikowski, Z. J., and Stec, W. J. New approach to the syntrhesis of nucleoside phosphorothioates. J Chem Soc Chem Commun. 1976: Adamiak, D. A.; Kinas, R.; Saenger, W., and Stec, W. J. Absolute Konfiguration des cancerostaticums S(-)cyclophosphamid (Cytoxan, Endoxa, NSC-26271). Angew Chem. 1977; 89: X-ray diffraction study and determination of absolute configuration of the anticancer drug S(-)cyclophosphamide (Endoxan, Cytoxan, NCS-26271). Z Naturforsch. 1977; 32c: Binkowski, J. and Giziński, S. Untersuchung der Absorption der bei der Verbrennung phosphororganischer Verbindungen enstehenden P-oxide mittels 32 P-markierten Verbindungen. II. Mikrochim Acta. 1977; II: Binkowski, J. and Rudnicki, A. Elementaranalyse phosphoroorganischer Verbindungen. VII. Phosphorbestimmung in selenhaltigen Substanzen. Mikrochim Acta. 1977: Brzezińska, K.; Chwiałkowska, W.; Kubisa, P.; Matyjaszewski, K., and Penczek, S. Ion-trapping in cationic polymerizations. Makromol Chem. 1977; 178: Chojnowski, J.; Cypryk, M.; Fortuniak, W., and Michalski, J. Methods of synthesis of O,O-bis(trimethylsilyl) phosphorothiolates. Synthesis. 1977: Chojnowski, J.; Wilczek, L., and Fortuniak, W. The mechanism of the hydride transfer from silicon to the carbonium ion in a weakly nucleophilic medium. J Organomet Chem. 1977; 135: Chojnowski, J.; Ścibiorek, M., and Kowalski, J. Mechanism of the formation of macrocycles during the cationic polymerization of cyclotrisiloxanes - end to end ring closure versus ring expansion. Makromol Chem. 1977; 178: Cox, P. J.; Farmer, P. B.; Foster, A. B.; Griggs, L. J.; Jarman, M.; Kinas, R.; Pankiewicz, K., and Stec, W. J. Application of deuterium labelling. Mass spectrometry in a study of the metabolism of the enantiomers of cyclophosphamide. Biomed Mass Spectrom. 1977; 4: Farmer, P. B.; Jarman, M.; Facchinetti, T.; Pankiewicz, K., and Stec, W. J. The metabolism and antitumor activity of the enantiomers of cis- and trans-4-methylcyclophosphamide. Chem Biological Interactions. 1977; 18: Gazicki, M.; Wróbel, A. M., and Kryszewski, M. Studies on soluble freaction of glow discharge polysilazane formed from hexamethylcyclotrisilazane. J Appl Polym Sci. 1977; 21: Gałdecki, Z.; Główka, M. L.; Michalski, J.; Okruszek, A., and Stec, W. J. P-Methyl-P-phenylpropylphosphine selenide. Acta Crystallogr. 1977; B33: Gałęski, A.; Kastelic, J.; Baer, E., and Kohn, R. R. Mechanical and structural changes in rat tail fendon induced by diabetes mellitus and aging. J Biomechanies. 1977; 18: Gałęski, A.; Milczarek, P., and Kryszewski, M. Heart conduction in two-dimensional spherulite. J Polym Sci B: Polym Phys. 1977; 15: Gałęski, A.; Pakuła, T., and Kryszewski, M. Small angle light scattering from helically twisted fibers. J Polym Sci Polym Symp. 1977; 61: Gogolczyk, W.; Słomkowski, S., and Penczek, S. Ion -pair dissociation equilibria for trityl AsF 6 - and SbF 6- in polar solvents. J Chem Soc Perkin : Kałużyński, K.; Libiszowski, J., and Penczek, S. Poly(2-hydro-2-oxo-1,3,2-dioxaphosphorinane). Preparation and NMR spectra. Makromol Chem. 1977; 178:2943.

14 227. Kinas, R.; Pankiewicz, K.; Stec, W. J.; Farmer, P. B.; Foster, A. B., and Jarman, M. Synthesis and absolute configuration of the optically active forms of 2-[bis(2-chloroethyl)amino]-4-methyltetrahydro-2-H-1,3,2-oxazaphosphorine 2-oxide(4-methylcyclophosphamide). J Org Chem. 1977; 42: Kowalski, J. and Lasocki, Z. Structure of disilylacetamides. J Organomet Chem. 1977; 128: Kowalski, J.; Ścibiorek, M., and Chojnowski, J. Correlation of the responce factors of thermal conductivity detector with molecular weight for methylsiloxanes versus ring expansion. J Chrom. 1977; 130: Krawczyk, E.; Michalski, J.; Pakulski, M., and Skowrońska, A. Novel five-coordinate phosphorus system via oxidative addition of pseudohalogens to organic phosphites. Tetrahedron Lett. 1977: Kubisa, P. Kinetics of nucleophilic substitution in the 1,3-dioxolan-2-ylium cation. Bull Pol Acad Sci Chem. 1977; Kinetics of polymerization of 1,3-dioxolan initiated by C 6H 5CO + SbF 6 and (C 6H 5) 3C + SbF 6 salts. J Macromol Sci Chem. 1977; A 11: Kubisa, P. and Penczek, S. 1 H NMR studies of the 1,3-dioxolan (C 2H 5) 3O + SbF 6 system, end groups and structure of the active species. Macromolecules. 1977; 10: Lesiak, K. and Stec, W. J. Synthesis of asymmetric S,S,S,-trialkyl phosphorotrithioates. Synthetic Commun. 1977: Matyjaszewski, K. and Penczek, S. Influence of concentration of living ends on the equilibrium between macroesters and macroions in the cationic polymerization of THF. J Polym Sci A: Polym Chem. 1977; 15: Mazurek, M. and Chojnowski, J. Anionic polymerization of siloxanes. II. Internal multifunctional assistance of siloxane system to the siloxane bond cleavage by alkali metal silanolates. Makromol Chem. 1977; 178: Michalski, J. New aspects of organophosphorus-sulphur chemistry. Synthesis of phosphinyl sulphenyl chlorides and their reactions as an example. I st International Congress on Phosphorus Compounds; Rabat. 1977: Michalski, J. and Skrzypczyński, Z. Novel reaction of phosphinothioic metanesulphonic anhydride with aluminium halides. Stereoselective synthesis of phosphonothioic halides. J Chem Soc Chem Commun. 1977: Mikołajczyk, M.; Bujnicki, B., and Drabowicz, J. Inversion of the sulphinamide configuration. Bull Pol Acad Sci Chem. 1977; XXV: Mikołajczyk, M.; Kiełbasiński, P.; Barlow, J. H., and Russell, D. R. Reaction between dithioacetic acid and dicyclohexyl-carbodiimide-structure of products. Crystal and molecular structure of trans-2,4-dimethyl-2,4-bis-thioacetylthio-1,3-dithietane. J Org Chem. 1977; 42: Mikołajczyk, M.; Kiełbasiński, P., and Goszczyńska, Z. Direct observation, isolation and structure of 1:1 adducts from carbodiimides and dialkyl phosphorothio(seleno)ic acids. J Org Chem. 1977; 42: Mikołajczyk, M.; Krzywa ński, J., and Ziemnicka, B. Stereochemistry of organophosphorus cyclic compounds. VI. Stereochemistry of the reaction between sulfenyl chlorides and trivalent phosphorus compounds. J Org Chem. 1977; 42: Mikołajczyk, M. and Witczak, M. Stereochemistry of organophosphorus cyclic compounds. V.

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