Micro-Raman System. Prezentacja oferty

Transkrypt

1 Micro-Raman System Prezentacja oferty

2 Cechy Różne długości fali laserów 532nm, 633nm & 785nm Niewielki rozmiar ogniska lasera < 1µm Dobra czułość Wiele trybów: Fluorescencja, polaryzacja DIC, Mikro-UV-VIS, pomiar ciemnego pola Niewielkie koszty utrzymania Polarization Raman (opcja) Mapowanie ramanowskie (opcja)

3 Elastyczność Akcesoria: Zautomatyzowany stolik Uchwyt na kuwety Grzany/chłodzony stolik Osłona zewnętrzna Tryby obrazowania: Bright-field Dark-field Phase-contrast Fluorescence Polarization UV-Vis spectroscopy

4 Graficzny interfejs

5 Konfiguracje

6 Konfiguracje 1. Długość fali lasera: 532nm, 633nm oraz 785nm (inne możliwe) 2. Chłodzone i niechłodzone 3. Z lub bez mikroskopu (wersja -M lub Ci) 4. Polaryzacja? Mapowanie? Osłona?

7 Intensity (cts) Intensity (cts) Konfiguracja długość fali Pojedyncza warstwa grafenu przy wzbudzeniu różnymi długościami fali lasera Laser wavelength D G cm Raman shift (cm -1 ) Raman shift (cm -1 )

8 Configuration - wavelength uraman-532 : (A) Range of cm-1 and Resolution ~10 cm-1 (B) Range of cm-1 and Resolution ~7 cm-1 (C) Range of cm-1 and Resolution ~5 cm-1 uraman-633 : (A) Range of cm-1 and Resolution ~7 cm-1 (B) Range of cm-1 and Resolution ~5 cm-1 uraman-785 : (A) Range of cm-1 and Resolution ~8 cm-1 (B) Range of cm-1 and Resolution ~4.5 cm-1 (C) Range of cm-1 and Resolution ~9 cm-1 (2x Signal of #B) UPG-CutOff : Upgrade for lower cut-off wavelength ur532 (from 95cm-1) ur633 (from 80cm-1) ur785 (from 80cm-1)

9 Niechłodzony: 1. Ekonomiczne rozwiązanie dla próbek o silnym sygnale Ramana 2. Tylko do szybkich pomiarów: do 5 sekund Konfiguracja chłodzenie? Chłodzony: 1. Do 10x mniejsze szumy tła 2. Do ogólnych zastosowań laboratoryjnych z różnorodnymi substancjami 3. Pomiary wymagają 10 sekund lub więcej 4. TEC do 5 o C (możliwe również osiągnięcie -5 o C)

10 Konfiguracja Mikroskop? Bez mikroskopu (dopasowanie do mikroskopu klienta): a) Jaki model/marka = Olympus, Zeiss, Leica, Nikon (inne możliwe) b) Tryby obrazowania/jakie są dostępne uchwyty c) Wymagane przesłanie fotografi w celu potwierdzenia d) Wymagana szczegółowa specyfikacja (jeżeli możliwe)

11 Konfiguracja - Mikroskop? Z mikroskopem: a) Oświetlenie transmisyjne i/lub refleksyjne b) Tryby obrazu = BF, DF, Phase, DIC, POL, Fluorescencja? c) Powiększenie = 2x, 4x/5x, 10x, 20x, 40/50x, 100x

12 Konfiguracja konfokalny Raman?

13 Key Specifications 1/2 1. Laser Spot down to 1um (based on 100x objective lens) Diffraction limit and dependence on NA of Lens 2. Single Mode Laser with narrow linewidth ; < 150 MHz (0.005cm -1 ) 3. Software continuously adjustable power (0.1mW step) 4. Raman Mapping (or upgradeable for) (75x50mm, 1um repeatability, 50nm step) 5. Polarization Raman (or upgradeable for) 6. Footprint (exclude computer): 500mm x 500mm, or smaller

14 Key Specifications 2/2 7. Microscope upgradeable with phase contrast, darkfield, DIC, fluorescence observation without sacrificing Raman performance 8. Performance (at <1um laser spot) [532]: Acquire G1 band of monolayer graphene samples with >5 SNR at 0.1sec integration and 1x averaging [633] : Acquire Polystyrene peak of 1001cm-1 with >100 SNR at 0.1sec integration time and 1x averaging [785]: Acquire Polystyrene peak of 1001cm-1 with >100 SNR at 0.1sec integration time and 1x averaging.

15 Customers (partial) International Clients Germany : Max Planck Institute for Polymer Research Spain : Centre Tecnològic de la Química de Catalunya Japan: Tokushima University Malaysia : Universiti Kebangsaan Malaysia (UKM) Singapore Institute of Materials Research and Engineering (IMRE) - A*STAR Institute of Molecular Biology (IMB) - A*STAR Nanyang Technological University (NTU), School of Physical and Mathematical Sciences National University of Singapore (NUS), Department of Bioengineering National University of Singapore (NUS), Department of Physics National University of Singapore (NUS), Physics Teaching Laboratory Temasek Lifescience Laboratory (TLL)

16 Testimonials (partial) Technospex offers a low cost and most importantly high quality Raman micro-spectrometer, the uraman, that easily competes with (and outperforms, in some cases) industry-standard systems. Our lab is very happy with the performance and flexibility of the system. An added benefit is the field-upgradability of the hardware and software a critical feature as we can quickly customize and add features for specific experiments with essentially zero downtime. Finally, the exceptional technical support from Technospex has made our experience with the uraman very productive. Dr. Sapun Parekh, Group Leader Max Planck Institute for Polymer Research Germany TechnoSpex s uraman small footprint was ideal for our undergraduate teaching lab, and the fully integrated yet simple design also allows our students to execute measurement easily. What really caught our initial interest was its ease in obtaining beautiful spectrum even from samples with monolayer thicknesses such as 2D materials, which our research labs are doing with systems costing much more. Thus far, the system has been performing very well and beyond our expectations. We are also very happy and impress by their attention to customer needs and the level of technical support provided in meeting our teaching lab demands. Dr TOK Eng Soon, Associate Professor Department of Physics National University of Singapore

17 Testimonials (partial) Technospex offers a low cost and most importantly high quality Raman micro-spectrometer, the uraman, that easily competes with (and outperforms, in some cases) industry-standard systems. Our lab is very happy with the performance and flexibility of the system. An added benefit is the field-upgradability of the hardware and software a critical feature as we can quickly customize and add features for specific experiments with essentially zero downtime. Finally, the exceptional technical support from Technospex has made our experience with the uraman very productive. Dr. Sapun Parekh, Group Leader Max Planck Institute for Polymer Research Germany TechnoSpex s uraman small footprint was ideal for our undergraduate teaching lab, and the fully integrated yet simple design also allows our students to execute measurement easily. What really caught our initial interest was its ease in obtaining beautiful spectrum even from samples with monolayer thicknesses such as 2D materials, which our research labs are doing with systems costing much more. Thus far, the system has been performing very well and beyond our expectations. We are also very happy and impress by their attention to customer needs and the level of technical support provided in meeting our teaching lab demands. Dr TOK Eng Soon, Associate Professor Department of Physics National University of Singapore

18 Publikacje (wybrane) Yang, Yijie, et al. "A Chemical Approach to Break the Planar Configuration Of Ag Nanocubes into Tunable Two-dimensional Metasurfaces." Nano letters (2016). He, Shuai, et al. "Optimizing gold nanostars as a colloid-based surface-enhanced Raman scattering (SERS) substrate." Journal of Optics (2015): Suresh, Vignesh, and Fung Ling Yap. "Flexible, transparent and robust SERS tapes through a two-step block copolymer self-assembly process." RSC Advances 5.76 (2015): Gao, Yu, et al. "Characterization of Titanium Dioxide Nanoparticles on Porcine Skin by Raman Microscopy." Analytical Letters (2015): Tan, Khay M., et al. "Toward the development of Raman spectroscopy as a nonperturbative online monitoring tool for gasoline adulteration." Analytical chemistry 85.3 (2013):

19 Applications (samples taken using uraman/usight-x)

20 Polarized Raman Polarized Raman of as received and stretch LDPE film Typical polarized Raman spectra of cyclohexane

21 Surface Enhanced Raman Scattering (SERS)

22 SERS - Superhydrophobic SERS platform with Methylene Blue as detection molecule 1 mm Methylene Blue (dye) on SERS substrate with different laser excitation wavelength

23 Gemstones Authenticity

24 Minerals / Gemstones

25 Biology Dermatology Dentistry Stem cell research Cancer studies Surgery etc

26 Biology Bacteria

27 Graphene 1 sec integration

28 Reflectance (%) Intensity (a.u.) Graphene - Raman + UV-Vis Micro-spectroscopy (i) (ii) (iii) 90 (iv) (i) (ii) (iii) (iv) 5000 Graphene 50 Taken with usight Wavelength (nm) Raman Shift (cm-1)

29 Stress mapping in semiconductor 149 x 133 pixels

30 Indentation and Material Stress mapping Peak intensity at 520cm -1 Peak FWHM Peak shift 3 1 2

31 Indentation and Material Stress mapping Peak intensity at 520cm -1 Peak FWHM Peak shift 2 1 3

32 Gasoline Adulteration Khay M Tan, et. al, Toward the Development of Raman Spectroscopy as a Nonperturbative Online Monitoring Tool for Gasoline Adulteration, Anal. Chem., 2013, 85 (3), pp